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Structural analysis and phase transition study of the compound Pb(x)Cd(1-x)TiO3: by X-ray diffraction and Raman spectroscopy This work aims to study the structural properties by X-ray diffraction (XRD) and Raman spectroscopy and phase transition, through vibrational spectra, of compounds of the type ABO3, specifically, ferroelectric materials of the type perovskite. The compounds PbTiO3 (PT), CdTiO3 (CT) and the cationic substitution at site A between these two materials were studied Pb(x)Cd(1-x)TiO3, in the concentrations of x = 1.0, 0.9, 0.8, 0.7, 0.6, 0.5, 0.4, 0.3, 0.2, 0.1 and 0.0. For each of these values, XRD and Raman measurements were performed. The synthesis was performed by the solid state reaction method, with modification of the reagents PbO and CdO, keeping the molarity of TiO2 constant. The new temperatures of synthesis of the compound were estimated by the Vegard equation. The PbTiO3, at room temperature, is a ferroelectric perovskite that has a tetragonal structure, while the CdTiO3 can be synthesized to have a rhombometric structure of the center-symmetric or orthorhombic perovskite type. However, the synthesis temperatures used in this work favor only the center-symmetrical ilmenite phase of the CT. It was found that the transition temperature of ferroelectric-paraelectric phase (Curie Temperature) of PT is ≈ 490°C. The CT, in its center-symmetric ilmenite phase, is stable at room temperature and at temperatures below 900°C. When replacing the oxides (PbO by CdO) between the lead and cadmium titanates, the transition temperature varies, as well as the other physical properties of the compound, giving rise to a new material. It was also observed that, at a certain concentration, the structural phases of the two titanates coexist, which indicates the possible formation of a particulate composite. Thus, it is possible to obtain a still ferroelectric material with a perovskite structure, with inherent characteristics of the CT, which has a center-symmetrical ilmenite structure. It was possible to analyze the phase transitions of these compounds through the peaks of soft mode (of lower frequency) in the Raman spectrum, with the atomic substitution in the structure of ion A and also through stimulus by temperature, determining the new temperatures phase transition for concentrations of x = 0.9, 0.5, 0.4, 0.2. PbTiO3 is used as a reference for the analysis of measurements, while CdTiO3 has the function of modifying the ferroelectric phase. It is important to highlight that this is a matter of convention, because while studying the changes that the CdO makes in the PbTiO3 phase, at the same time we study the changes that the PbO makes in the structure of CdTiO3. Due to the versatility of the perovskite structure, a material used in several technological applications, the study of these materials and their different configurations is relevant in order to map and identify their potential and possible implementations.